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US Patent 7213325 Method of manufacturing Fe-sheathed MgB2 wires and solenoids

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Patent
Patent

Patent attributes

Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
Patent Number
7213325
Patent Inventor Names
Kamel Salama0
Hui Fang0
Date of Patent
May 8, 2007
Patent Application Number
11050186
Date Filed
February 3, 2005
Patent Primary Examiner
‌
Carl J. Arbes
Patent abstract

A method of manufacturing a Fe-sheathed MgB2 wire includes the steps of:I. Selecting a carbon steel tube with 0.1% to 0.3% carbon;a. Crimping a first end of the tube;b. Selecting a Mg powder at least 99.8% pure, and sized for 325 mesh;c. Selecting a B powder, at least 99.99% pure, and sized for 325 mesh;d. Stoichiometrically mixing the Mg and B powders to form a mixture powder;e. Milling the mixture powder by using high-energy ball mill for 0.5 to 6 hours and using stainless steel mixing balls and vial, wherein the mass ratio of ball to powder is 20:1, to form a milled powder;f. Filling and packing the tube in an argon atmosphere with the milled powder to create a packing density of about 1.5 g/cm3;g. Crimping the second end of the tube to create a powder-filled tube;h. Rolling the powder-filled tube to create the Fe-sheathed MgB2 wire; andi. Annealing the as-rolled wire at 600 to 900° C. for 0.5 to 3 hours at high purity argon environment to create superconducting wire.

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