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US Patent 7547803 Process for producing a high purity aromatic polycarboxylic acid

Patent 7547803 was granted and assigned to Mitsubishi Gas Chemical Company on June, 2009 by the United States Patent and Trademark Office.

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Patent
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Patent attributes

Current Assignee
Mitsubishi Gas Chemical Company
Mitsubishi Gas Chemical Company
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Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
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Patent Number
75478030
Patent Inventor Names
Shinichi Nagao0
Jitsuo Oishi0
Kenji Nakaya0
Masato Inari0
Hiroshi Machida0
Date of Patent
June 16, 2009
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Patent Application Number
108614970
Date Filed
June 7, 2004
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Patent Primary Examiner
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Taylor Victor Oh
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Patent abstract

A process for producing a high purity aromatic polycarboxylic acid (APA) by purification of a crude APA comprises: (I) aging a slurry of the crude APA in a first dispersion medium at 180 to 300° C. for 10 minutes or longer under stirring; (II) introducing the aged slurry of the APA into a column for substituting dispersion media, bringing the slurry into contact with a second dispersion medium and separating the resultant fluid into a fluid of the first dispersion medium containing impurities and a slurry of the second dispersion medium containing crystals of the high purity APA; and (III) separating the crystals of the high purity APA from the slurry of the second dispersion medium. A high purity APA having excellent hue and particle diameter can be industrially advantageously produced while the construction of the process is simplified and the consumption of energy is decreased.

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