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US Patent 9028724 Method for preparing water-soluble nanoparticles and their dispersions

Patent 9028724 was granted and assigned to Hanwha Chemical on May, 2015 by the United States Patent and Trademark Office.

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Current Assignee
Hanwha Chemical
Hanwha Chemical
Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
Patent Number
9028724
Date of Patent
May 12, 2015
Patent Application Number
13395827
Date Filed
September 14, 2010
Patent Citations Received
‌
US Patent 12128612 Binder agent
0
Patent Primary Examiner
‌
Mark Kopec
Patent abstract

Provided is a method for preparing an aqueous dispersion of metal nanoparticles having superior dispersibility and being sinterable at low temperature by modifying the surface of metal nanoparticles having hydrophobic groups with hydrophilic groups. Specifically, by treating the surface hydrophobic groups of the metal nanoparticles with a surface modification solution containing a surfactant and a wetting-dispersing agent, the treatment throughput can be improved about 10-fold and the particles can be monodispersed without agglomeration. Further, by using an antioxidant and a ligand removal agent in the solution, denaturation and oxidation of the particles can be prevented and the high-boiling-point hydrophobic ligands can be eliminated effectively. The hydrophilically treated metal nanoparticles may be dispersed in an aqueous-based solvent to prepare a metal ink sinterable at low temperature.

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