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US Patent 9517945 Low-temperature route for precision synthesis of metal oxide nanoparticles

Patent 9517945 was granted and assigned to University of Oregon on December, 2016 by the United States Patent and Trademark Office.

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Patent
Patent

Patent attributes

Patent Applicant
University of Oregon
University of Oregon
Current Assignee
University of Oregon
University of Oregon
Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
Patent Number
9517945
Date of Patent
December 13, 2016
Patent Application Number
14092800
Date Filed
November 27, 2013
Patent Citations Received
‌
US Patent 12134566 Method for producing indium tin oxide particles and method for producing curable composition
0
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US Patent 11975390 Method for producing indium tin oxide particles and method for producing curable composition
0
Patent Primary Examiner
‌
Richard M Rump
Patent abstract

Methods for making metal oxide nanoparticles, including mixed metal oxides and core-shell metal oxide nanoparticles, are disclosed. A solution comprising a metal carboxylate and a carboxylic acid is combined with a solvent comprising an alcohol heated to a temperature ≦250° C. for an effective period of time to form metal oxide nanoparticles. The metal may be a group IIIA metal, a group IVA metal, a transition metal, or a combination thereof. A metal oxide shell may be deposited onto metal oxide nanoparticles by dispersing the metal oxide nanoparticles in an alcohol, adding a metal carboxylate, and maintaining the reaction at a temperature ≦200° C. for an effective period of time to form core-shell nanoparticles. The nanoparticles may have a relative size dispersity of ≦20%, and may further comprise a plurality of carboxylic acid, carboxylate, and/or alcohol ligands coordinated to the nanoparticles' outer surfaces.

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